Continuous in situ generation and reaction of phosgene in a microflow system.
نویسندگان
چکیده
Continuous in situ generation of phosgene and its use in acid chloride formation in a microflow system were demonstrated. The acid chloride was subsequently coupled with an amine in high yield without severe epimerization.
منابع مشابه
In situ electrogeneration of o-benzoquinone and high yield reaction with benzenethiols in a microflow system.
We have successfully demonstrated that a microflow reactor is extremely useful in controlling reactions involving an unstable o-benzoquinone. The key features of the method are an effective o-benzoquinone generation and its rapid use for the following reaction without decomposition in a microflow system.
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ورودعنوان ژورنال:
- Chemical communications
دوره 47 47 شماره
صفحات -
تاریخ انتشار 2011